Analytical chemistry Part II Quantitative analysis

“Analytical chemistry Part II Quantitative analysis By Valeriy V. Bolotov, Tatyana A. Kostina, S. V. Kolisnyk Book Free Download”

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Table Of Content:

Subject and problems of quantitative analysis ………………………………………3
Classification of quantitative analysis methods ……………………………………3
Gravimetric method of analysis ………………………………………………………….5
Precipitation methods ………………………………………………………5
Volatilization methods ……………………………………………………..6
Particulate methods …………………………………………………………7
Balance and weighing technique ……………………………………….8
Equipment and technique of carrying out the basic
operations …………………………………………………………………….15
Calculations in gravimetric methods of analysis………………………….20
Laboratory works ………………………………………………………….22
Control questions for in-class and out-of-class work
of students ……………………………………………………………………………..30
Titrimetric methods of analysis …………………………………………………………32

Classification of titrimetric methods of analysis
according to types of chemical reactions …………………………..33
Classification of titrimetric methods according
to the way of titration ……………………………………………………..33
Technique and accuracy of analysis …………………………………34
Measuring the volumes of solutions …………………………………36
Calculations in titrimetric methods of analysis ……………………………41
General statements of titrimetry ………………………………………41
The expression ways of solutions concentration ………………..43
The calculation formulae in titrimetric analysis …………………45
The general rules of filling the laboratory register ……………..52
Laboratory works ………………………………………………………….53
The acid-base titration (the neutralization method) ……………………………..57
Laboratory works ………………………………………………………….59
Control questions for in-class and out-of-class work
of students ……………………………………………………………………………..69
Titrimetric methods of precipitation (the precipitation titration) ……………70
Argentometry …………………………………………………………………………70
The Mohr method ……………………………………………………………..71
Laboratory works ………………………………………………………….72

The Fajans-Khodakov method ……………………………………………74
Laboratory works ………………………………………………………….76
Thiocyanatometry (rodanometry). The Folgard method …………77
Laboratory works ………………………………………………………….80
Mercurometry ………………………………………………………………………..83
Laboratory works ………………………………………………………….84
Control questions for in-class and out-of-class work
of students ……………………………………………………………………………..87
Methods of complex formation (complexometry) ……………………………….89
Mercurimetric titration …………………………………………………………….89
Laboratory works ………………………………………………………….91
Complexonometry (trilonometry) ……………………………………………..93
Laboratory works ………………………………………………………….96
Control questions for in-class and out-of-class work
of students ……………………………………………………………………………..99
The oxidation-reduction titration ……………………………………………………. 100
Permanganatometry ……………………………………………………………… 106
Laboratory works ……………………………………………………….. 108
Bromatometry ……………………………………………………………………… 114
Laboratory works ……………………………………………………….. 115
Chromatometry ……………………………………………………………………. 118
Laboratory works ……………………………………………………….. 119
Iodometry ……………………………………………………………………………. 121
Laboratory works ……………………………………………………….. 127
Iodochlorimetry ……………………………………………………………………. 137
Laboratory works ……………………………………………………….. 139
Cerimetry ……………………………………………………………………………. 144
Laboratory works ……………………………………………………….. 145
Nitritometry …………………………………………………………………………. 148
Laboratory works ……………………………………………………….. 150
Control questions for in-class and out-of-class work
of students

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